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Metal Mine ›› 2019, Vol. 48 ›› Issue (03): 90-94.

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Experiment on Reduction and Extraction of Nickel from High-magnesium Low-iron Nickel Laterite by Rotary Hearth Furnace

Wang Jingjing1,2,Cao Zhicheng1,2,Gao Jianyong1,2,Yan Kun1,2   

  1. 1. Beijing Shenwu Environment & Energy Technology Co.,Ltd, Beijing 102200,China;2.Beijing Comprehensive Utilization of Low-Grade Iron Ore, Engineering and Technology Research Center, Beijing 102200,China
  • Online:2019-03-25 Published:2019-04-30

Abstract: The low-iron, low-nickel and high-magnesium nickel laterite ore was investigated, in which contains 17.68% iron, 1.62 nickel and 19.06% MgO, respectively. Nickel mainly replaces iron and magnesium and exists in the form of isomorphism in iron oxides and silicate minerals, accounting for 39.65% and 54.72%. To determine the high-efficiency development utilization process, small-scale basic tests were conducted to obtain the parameters of the reduction-roasting and grinding-separation process and pilot-scale test was carried out on a rotary hearth furnace with a pitch diameter of 8 m. The results showed that the sample was treated by coal-based direct reduction, water quenching and two-stage grinding and low-intensity magnetic separation. The mass ratio of laterite nickel ore, limestone and TN was 100∶10∶3, mole ratio of C to O was 1.2 (anthracite) , the reduction time was lasted 40 min in the temporary of 1 280 ℃. The water-quenched calciation products at first stage grinding fineness of -0.074 mm accounting for 83.31%, and the magnetic field intensity of first stage low-intensity magnetic separation was 190.98 kA/m, second stage grinding fineness of -0.074 mm accounting for 97.43%, and the magnetic field intensity of second stage low-intensity magnetic separation was 127.32 kA/m. Under the optimal conditions, ferronickel powder product which contains 5.63% nickel and 60.39% iron with recovery of 80.83% and 75.14% can be obtained. The pilot product of the rotary hearth furnace was ground and separated. The obtained ferronickel powder product contains 5.26% nickel and 59.20% iron, while the recovery of nickel and iron were 80.84% and 74.98%, respectively. The research results can be used as the basis for engineering, and can also provide a technical reference for the efficient development and utilization of the same type of laterite nickel ore resources.

Key words: Nickel laterite ore, rotary hearth furnace, direct reduction, grinding, low-intensity magnetic separation