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金属矿山 ›› 2021, Vol. 50 ›› Issue (07): 142-145.

• 矿物工程 • 上一篇    下一篇

鞍钢某铁尾矿磁化焙烧—磁选试验研究

张  毅1,2  余  莹 张五志1,2  高  鹏1,2
  

  1. 1. 东北大学资源与土木工程学院,辽宁 沈阳 110819;2. 难采选铁矿资源高效开发利用技术国家地方联合工程研究中心,辽宁 沈阳 110819;3. 鞍钢集团矿业弓长岭有限公司选矿分公司,辽宁 辽阳 111008
  • 出版日期:2021-07-15 发布日期:2021-08-06
  • 基金资助:
    国家自然科学基金项目(编号:51734005);中央高校基本科研业务专项资金资助项目(编号:N182508026)

Experimental Study on Magnetization Roasting and Magnetic Separation of an Iron Tailings in Ansteel

ZHANG Yi1,2    YU Ying3    ZHANG Wuzhi1,2    GAO Peng1,2   

  1. 1. School of Resources and Civil Engineering, Northeastern University, Shenyang 110819, China; 2. National-Local Joint Engineering Research Center of Refractory Iron Ore Resources Efficient Utilization Technology, Shenyang 110819, China;3. Gongchangling Concentrator, Gongchangling Mine Industry Company, Ansteel Group, Liaoyang 111008, China
  • Online:2021-07-15 Published:2021-08-06

摘要: 为了确定适宜的磁化焙烧条件,采用磁化焙烧—磁选工艺,对鞍钢某铁尾矿进行了系统的试验研究,考察了焙烧温度、焙烧时间、还原气体浓度以及气体流速对磁化焙烧效果的影响,结果表明:①鞍钢铁 尾矿TFe品位为14.70%,主要杂质SiO2含量为66.17%,有害元素P、S、Na的含量较少;铁尾矿中的铁主要以赤、褐铁矿的形式存在,分布率为83.87%;铁尾矿中主要有用矿物为磁铁矿、赤铁矿,主要脉石矿物为石英。 ②该铁尾矿适宜的焙烧条件为:焙烧温度580 ℃、焙烧时间5 min、CO浓度30%、气体流速500 mL/min;在此条件下获得的焙烧产品,经弱磁选(磁场强度为87.12 kA/m)选别,可获得TFe品位62.17%、TFe回收率 84.02%的磁选精矿。③焙烧产品的铁物相分析结果表明,经过磁化焙烧,试样中磁性铁的含量和分布率显著提高,赤、褐铁矿中的铁含量和分布率则大幅度降低。不同焙烧时间下产品的XRD谱图结果进一步说明铁尾矿 中的赤铁矿转换成了磁铁矿。研究结果可为同类型尾矿的开发利用提供参考。

关键词: 铁尾矿, 磁化焙烧, 磁选, 赤褐铁矿, 磁铁矿

Abstract: In order to determine the suitable conditions of magnetization roasting, the process of magnetization roasting and magnetic separation was adopted to conduct a systematic experimental study on an iron tailings from Anshan Iron and Steel Company. The Influence of roasting temperature, roasting time, reducing gas concentration and gas flow rate on the effect of magnetization roasting were investigated. The results showed that: ① The TFe grade of Anshan iron tailings is 14.70% and the main impurity SiO2 contents is 66.17%. The contents of harmful elements, such as phosphorus, sulfur and sodium are less. The iron in the iron tailings mainly exists in the form of hematite and limonite, with the distribution rate of 83.87%. The main useful minerals in the iron tailings are magnetite and hematite, and the main gangue mineral is quartz. ② The suitable roasting conditions of the iron tailings are as follows: roasting temperature of 580 ℃, roasting time of 5 min, CO concentration of 30%, gas flow rate of 500 mL/min. Under the suitable conditions, magnetic concentrate with TFe grade of 62.17% and TFe recovery rate of 84.02% was obtained by low intensity magnetic separation of the roasted products with the magnetic field intensity of 87.12 kA/m. ③ The results of iron phase analysis of roasted products showed that the contents and distribution of magnetic iron in the samples were significantly increased after magnetization roasting, while the contents and distribution of iron in hematite and limonite were significantly decreased. The results of XRD patterns of products with different calcination time further indicate that hematite in iron tailings is transformed into magnetite. The research results could provide reference for the development and utilization of tailings of the same type.

Key words: iron tailings, magnetization roasting, magnetic separation, hematite and limonite, magnetite