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金属矿山 ›› 2025, Vol. 55 ›› Issue (8): 57-63.

• 矿物工程 • 上一篇    下一篇

基于矿物自动分析系统的红土镍矿酸浸渣的工艺 矿物学研究 

董再蒸1,2,3   孙永升1,2   齐赛男4   李鎏灿4   孙洪硕3   温利刚1,5   

  1. 1. 东北大学资源与土木工程学院,辽宁 沈阳 110819;2. 矿物加工科学与技术全国重点实验室,辽宁 沈阳 110819; 3. 酒泉钢铁(集团)有限责任公司,甘肃 嘉峪关 735100;4. 中色创新研究院(天津)有限公司,天津 300393; 5. 矿冶科技集团有限公司矿冶过程智能优化制造全国重点实验室,北京 100160
  • 出版日期:2025-09-15 发布日期:2025-09-15
  • 通讯作者: 温利刚(1992—),男,工程师,博士研究生。
  • 作者简介:董再蒸(1984—),男,高级实验师,博士。
  • 基金资助:
    辽宁省自然科学基金联合基金面上项目(编号:2023-MSBA-118);中央高校基本科研业务费专项(编号:N2401010);中国有色集团技 术攻关项目(编号:2022_2_KJJH01)。 

Mineralogy Research on Acid Leaching Residue of Laterite Nickel Ore Based on Mineral Automatic Analysis System 

DONG Zaizheng 1,2,3   SUN Yongsheng 1,2   QI Sainan 4   LI Liucan 4   SUN Hongshuo 3   WEN Ligang 1,5    

  1. 1. School of Resources and Civil Engineering,Northeastern University,Shenyang 110819,China;2. State Key Laboratory of Mineral Processing,Shenyang 110819,China;3. Jiuquan Iron & Steel (Group) Co. ,Ltd. ,Jiayuguan 735100,China; 4. China Nonferrous Metals Innovation Institute (Tianjin) Co. ,Ltd. ,Tianjin 300393,China;5. State Key Laboratory of Intelligent Optimized Manufacturing in Mining & Metallurgy Process,BGRIMM Technology Group,Beijing 100160,China
  • Online:2025-09-15 Published:2025-09-15

摘要: 为深入探究某红土镍矿高压硫酸酸浸渣的矿物组成、主要矿物的嵌布特征及元素的赋存形式,明确有 价金属回收及有害杂质分离的方法,对样品开展了工艺矿物学研究,分别采用化学多元素分析、化学物相分析和 SEMEDS-BPMA 矿物自动定量分析等手段对样品的化学组成、粒度特性、元素分布和矿物嵌布特征进行了详细分析。 研究 结果表明,样品中富含铁、铝等具回收价值的元素,其矿物重构程度高,主要矿物包括铁氧化物、铝钾硫铁氧化物、磁/ 赤铁矿及铬铁尖晶石类矿物。 样品粒度极细,-0. 010 μm 的含量高达 77. 56%,主要矿物的粒度绝大多数在 0. 038 μm 以下;铁氧化物单体含量高,与其他主要矿物的连生关系紧密。 由于铁、硫、铝元素均主要赋存在铁氧化物中,因此铁 与其他元素分离难度较大。 研究为此冶金次生固废高效利用方案的制定提供了重要的矿物学依据。 

关键词: 红土镍矿酸浸渣  工艺矿物学  自动分析  嵌布关系  元素赋存状态

Abstract: In order to further investigate the mineral composition,main mineral distribution characteristics,and element occurrence forms of high-pressure sulfuric acid leaching residue of laterite nickel ores,and clarify suitable methods for valuable metal recovery and harmful impurity separation,process mineralogy research was conducted on the sample. Chemical multi-element analysis,chemical phase analysis,and SEM-EDS-BPMA mineral automatic quantitative analysis were used to analyze the chemical composition,particle size characteristics,element distribution,and mineral distribution characteristics of the sample in detail. The research results indicated that the acid leaching residue of laterite nickel ore is rich in elements with recycling value such as iron and aluminum,and has a high degree of mineral reconstruction. The main minerals include iron oxides,aluminum potassium sulfide iron oxides,magnetite / hematite,and chromite spinel minerals. The sample has extremely fine particle size, with a content of up to 77. 56% at -0. 010 μm,and the majority of the main minerals have particle sizes below 0. 038 μm;Iron oxide monomers have a high content and are closely associated with other major minerals. Due to the fact that iron,sulfur,and aluminum elements are mainly present in iron oxides,it is difficult to separate iron from other elements. The study provides important mineralogical basis for the development of efficient utilization schemes for such metallurgical secondary solid waste. 

Key words: acid leaching residue of laterite nickel ore,process mineralogy,automatic analysis,embedding relationship, , assignment state of elements 

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