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金属矿山 ›› 2008, Vol. 38 ›› Issue (06): 45-48.

• 矿物工程 • 上一篇    下一篇

用微波还原—弱磁选工艺从包钢稀土尾矿回收铁

李保卫,张邦文,赵瑞超,李解   

  1. 内蒙古科技大学
  • 收稿日期:2008-04-05 出版日期:2008-06-15 发布日期:2011-07-18
  • 基金资助:

    内蒙古优秀学术带头人项目(编号:20060702),包头市重大科技攻关项目(编号:2006Z1004)。

Iron Recovery from Baosteel Rare Earth Flotation Tailings by Microwave Reduction-Magnetic Separation

Li Baowei,Zhang Bangwen,Zhao Ruichao,Li Jie   

  1. Inner Mongolia University of Science and Technology
  • Received:2008-04-05 Online:2008-06-15 Published:2011-07-18

摘要: 以微米炭、纳米炭为还原剂,进行了用微波还原—弱磁选工艺回收包钢稀土浮选尾矿中铁的试验研究。结果表明:在570 ℃下进行微波炭热处理后,尾矿中大部分赤铁矿被还原为磁铁矿,还原率超过85%;用纳米炭作还原剂时,微波加热速度远远快于用微米炭,炭粉用量也远比后者少;在纳米炭质量分数为0.8%、微波还原输入电压为220 V、还原矿球磨5 min、弱磁选磁感应强度为0.15 T的条件下,包钢稀土浮选尾矿经微波还原和1次弱磁选,可获得品位为63.00%、回收率为54.80%的铁精矿,并使稀土和铌在弱磁选尾矿中富集。

关键词: 包钢稀土浮选尾矿, 微波还原, 纳米炭, 弱磁选

Abstract: An experimental study was conducted on the iron recovery from the tailings of BaoSteel rare-earth flotation by microwave carbothermic reduction plus magnetic separation. At a temperature below 570 ℃, more than 85% of the hematite in the tailings was reduced into magnetite . It was found that nanocarbon particles when used as the reducer can have a much greater heating rate than that of microcarbon particles , with the carbon dosage also far less than that of the latter. In the case of C=0.8% (mass fraction of nanocarbon), U=220 V (microwave reduction input voltage) and B =0.15 T (magnetic induction intensity of low intensity magnetic separation, LIMS), an iron concentrate can be obtained from the tailing with a grade of 63% and a recovery of 54.80%  by microwave reduction and one pass LIMS, with the rare-earth and niobium enriched in LIMS tailings.

Key words: BaoSteel rare-earth flotation tailings, Microwave reduction, Nanocarbon, LIMS