Abstract: There is 0.11% Cu，1.16% S，0.22 WO₃ in a copper-tungsten polymetallic ore.Scheelite and chalcopyrite are mainly fine disseminated in the ore，79.55% scheelite distributed in 0.01 ~ 0.3 mm fraction，while 81.83% chalcopyrite distributed in 0.01~0.3 mm fraction.To provide technique basis for the development and utilization of the ore，on the basis of ore properties analysis，copper and sulphur bulk flotation-copper and sulphur separation flotation on the bulk flotation concentrate，tungsten flotation on the bulk flotation tailings was conducted.The results indicated that: at the grinding fineness of 65% passing 0.074 mm，using sodium silicate as the inhibitor，SN-9 as collector，BK201 as foaming agent，by one roughing-three cleaning-two scavenging copper and sulphur bulk flotation，bulk flotation concentrate using lime as inhibitor，Z-200 as collector，by one roughing-four cleaning-two scavenging copper and sulphur separation flotation，bulk flotation tailings using sodium carbonate as regulator，sodium silicate as inhibitor，W-1205 as collector，by one roughing-three cleaning-three scavenging flotation at normal temperature，flotation concentrate via one roughing-five cleaning-two scavenging flotation at 90 ℃，copper concentrate with 24.13% Cu and recovery 68.90%，sulfur concentrate with 36.15% S and recovery of 60.77%，and tungsten concentrate with 62.24% WO3 and recovery of 73.68%，were obtained.The test result is satisfactory，and can be used as technical basis for the development and utilization of the copper tungsten polymetallic ore.

Key words: Polymetallic complex ore, Chalcopyrite, Scheelite, Pyrite, Flotation